The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 05, 2016

Filed:

Aug. 05, 2014
Applicant:

Asiacom Group Investments, Inc., Oklahoma City, OK (US);

Inventors:
Assignee:

ASIACOM GROUP INVESTMENTS, INC., Oklahoma City, OK (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C10L 10/02 (2006.01); C07F 15/02 (2006.01); C07D 413/12 (2006.01); C07D 273/02 (2006.01); C07D 498/08 (2006.01); C09K 8/58 (2006.01); C10M 159/18 (2006.01); C09K 8/00 (2006.01); C10M 139/06 (2006.01); C10L 1/30 (2006.01);
U.S. Cl.
CPC ...
C10L 10/02 (2013.01); C07D 273/02 (2013.01); C07D 413/12 (2013.01); C07D 498/08 (2013.01); C07F 15/025 (2013.01); C09K 8/00 (2013.01); C09K 8/58 (2013.01); C10L 1/301 (2013.01); C10M 139/06 (2013.01); C10M 159/18 (2013.01); C09K 2208/10 (2013.01); C10L 2200/024 (2013.01); C10L 2230/14 (2013.01); C10M 2227/09 (2013.01); C10N 2220/082 (2013.01); C10N 2230/02 (2013.01); C10N 2230/12 (2013.01);
Abstract

A stabilized nano-Fe-iron-crown ether complex is added to a heavy oil to reduce the viscosity of the heavy oil. The complex may be formed by preparing a solution of an iron salt and an oligomer crown compound in dialkylamine or diethylamine. Sodium tetrahydroboron (NaBH) and dialkylamine or ethylendiamine are added at a temperature of 0-10° C. The mixture is heated to room temperature and boiled, thereby converting the formed iron (II)-borhydride complex (Fe(BH)) to a crown ether—iron-hydride complex [CWFe].(2H). At higher temperature this last complex is converted to the Fe-crown nanocomposite complex. The prepared nanoparticle Fe° complex may be stabilized by inclusion into a cavity of a macrocyclic compound, and may be (1) added to diesel fuel to reduce NOx emissions upon combustion of that fuel; (2) added to lubricating oils as an anticorrosion additive; and (3) used as an additive to secondary recovery processes within liquid hydrocarbon formations to increase the sweep efficiency and recovery factor of water-flooding operations.


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