The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 14, 2016

Filed:

Dec. 27, 2012
Applicants:

Asymchem Laboratories (Tianjin) Co., Ltd, Teda Tianjin, CN;

Asymchem Life Science (Tianjin) Co., Ltd, Teda Tianjin, CN;

Tianjin Asymchem Pharmaceutical Co., Ltd, Teda Tianjin, CN;

Asymchem Laboratories (Fuxin) Co., Ltd, Liaoning, CN;

Jilin Asymchem Laboratories Co., Ltd, Jilin, CN;

Inventors:

Hao Hong, Tianjin, CN;

James Gage, Tianjin, CN;

Chaoyong Chen, Tianjin, CN;

Jiangping Lu, Tianjin, CN;

Yan Zhou, Tianjin, CN;

Shuangyong Liu, Tianjin, CN;

Attorney:
Int. Cl.
CPC ...
C07D 475/04 (2006.01); C07D 239/50 (2006.01); C07D 239/48 (2006.01); C07D 239/47 (2006.01); C07D 303/48 (2006.01); C07D 317/26 (2006.01); C07D 317/28 (2006.01); C07D 317/32 (2006.01); C07C 209/62 (2006.01); C07C 221/00 (2006.01); C07C 225/06 (2006.01); C07D 301/03 (2006.01); C07D 301/12 (2006.01); C07D 301/14 (2006.01);
U.S. Cl.
CPC ...
C07D 475/04 (2013.01); C07C 221/00 (2013.01); C07D 239/50 (2013.01); C07D 301/03 (2013.01); C07D 301/12 (2013.01); C07D 301/14 (2013.01); C07D 317/26 (2013.01); C07D 317/28 (2013.01); C07D 317/32 (2013.01);
Abstract

Disclosed is a method for synthesizing sapropterin dihydrochloride. The present disclosure reduces a synthesis route of the sapropterin dihydrochloride, introduces a chiral center in an asymmetric synthesis manner, in which a tetrahydrofuran solution containing a samarium catalyst is adopted as a catalyst, and obtains a target compound having a high antimer isomerism value by means of selective catalysis. The yield is improved, raw materials are cheap and readily available, and the cost is significantly reduced, hence providing an effective scheme for mass industrial production of the sapropterin dihydrochloride.


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