The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 10, 2016

Filed:

Oct. 23, 2012
Applicants:

Bacock & Wilcox Technical Services Y-12, L.l.c., Oak Ridge, TN (US);

Fisk University, Nashville, TN (US);

Inventors:

Ashley Stowe, Knoxville, TN (US);

Arnold Burger, Nashville, TN (US);

Assignees:

Consolidated Nuclear Security, LLC, Reston, VA (US);

Fisk University, Nashville, TN (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C30B 11/08 (2006.01); C30B 11/12 (2006.01); C30B 29/46 (2006.01);
U.S. Cl.
CPC ...
C30B 11/12 (2013.01); C30B 29/46 (2013.01);
Abstract

A method for synthesizing I-III-VIcompounds, including: melting a Group III element; adding a Group I element to the melted Group III element at a rate that allows the Group I and Group III elements to react thereby providing a single phase I-III compound; and adding a Group VI element to the single phase I-III compound under heat, with mixing, and/or via vapor transport. The Group III element is melted at a temperature of between about 200 degrees C. and about 700 degrees C. Preferably, the Group I element consists of a neutron absorber and the group III element consists of In or Ga. The Group VI element and the single phase I-III compound are heated to a temperature of between about 700 degrees C. and about 1000 degrees C. Preferably, the Group VI element consists of S, Se, or Te. Optionally, the method also includes doping with a Group IV element activator.


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