The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 12, 2016

Filed:

Feb. 15, 2010
Applicants:

Atsushi Nomura, Sakai, JP;

Kenichi Nakagawa, Sakai, JP;

Takanori Morita, Sakai, JP;

Inventors:

Atsushi Nomura, Sakai, JP;

Kenichi Nakagawa, Sakai, JP;

Takanori Morita, Sakai, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C09D 17/00 (2006.01); B82Y 30/00 (2011.01); C01G 23/053 (2006.01);
U.S. Cl.
CPC ...
C09D 17/008 (2013.01); B82Y 30/00 (2013.01); C01G 23/053 (2013.01); C01G 23/0536 (2013.01); C01P 2002/72 (2013.01); C01P 2004/64 (2013.01); C01P 2006/12 (2013.01); C01P 2006/37 (2013.01); Y10T 428/2982 (2015.01);
Abstract

The invention provides a dispersion of particles of rutile titanium oxide wherein the particles of rutile titanium oxide have a D50 in a range of 1 to 15 nm and a D90 of 40 nm or less in particle size distribution as determined by a dynamic light scattering method; a specific surface area in a range of 120 to 180 m/g as determined by a BET method; and a rate of weight loss of 5% or less as obtained by heating the particles of rutile titanium oxide from 105° C. to 900° C. Such a dispersion of particles of rutile titanium oxide is obtained by a process according to the invention, which comprises: a first step in which an aqueous titanium tetrachloride solution is heated and hydrolyzed to obtain a slurry containing the precipitated particles of rutile titanium oxide; a second step in which the slurry obtained in the first step is filtered and washed with water to remove water-soluble salts dissolved therein from the slurry; a third step in which the slurry obtained in the second step is subjected to a hydrothermal reaction in the presence of an organic acid; a fourth step in which the slurry obtained in the third step is filtered and washed with water; a fifth step in which an acid is added to the slurry obtained in the fourth step, and the resulting mixture is subjected to a wet dispersion treatment, thereby obtaining a dispersion; and a sixth step in which excess acid and water-soluble salts are removed from the dispersion obtained in the fifth step.


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