The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 29, 2015

Filed:

Jul. 03, 2013
Applicant:

Segetis, Inc., Golden Valley, MN (US);

Inventors:

Brian D. Mullen, Delano, MN (US);

Leo E. Manzer, Wilmington, DE (US);

Cora M. Leibig, Maple Grove, MN (US);

Assignee:

SEGETIS, INC., Golden Valley, MN (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 69/66 (2006.01); C07C 69/738 (2006.01); C07C 51/09 (2006.01); C07C 51/493 (2006.01); C07C 67/08 (2006.01); C07C 67/52 (2006.01); C07C 69/716 (2006.01);
U.S. Cl.
CPC ...
C07C 69/738 (2013.01); C07C 51/09 (2013.01); C07C 51/493 (2013.01); C07C 67/08 (2013.01); C07C 67/52 (2013.01); C07C 69/716 (2013.01);
Abstract

Ketocarboxylic acids such as levulinic acid can be efficiently purified in high yield by esterification with a hydrocarbon polyol to the corresponding polyketocarboxylic ester, which can be readily purified, for example recrystallized. After purification, the ketocarboxylic ester can be hydrolyzed to provide pure ketocarboxylic acid, or a salt thereof, after removal of the esterifying hydrocarbon polyol, or used for other synthetic transformations. Advantageously, the polyketocarboxylic esters, ketocarboxylic acids, and salts thereof produced by this method are obtained in high purity.


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