The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 15, 2015

Filed:

Oct. 09, 2013
Applicant:

3m Innovative Properties Company, St. Paul, MN (US);

Inventors:

Steven J. Martin, Shoreview, MN (US);

Luke T. Dressel, Somerset, WI (US);

Aaron E. Hutt, St. Paul, MN (US);

Eric A. Schotz, Woodbury, MN (US);

Terence D. Spawn, Stillwater, MN (US);

Miguel A. Guerra, Woodbury, MN (US);

Tatsuo Fukushi, Woodbury, MN (US);

Jeremy A. Miller, Eagan, MN (US);

Christopher M. Geise, St. Paul, MN (US);

James A. McDonell, Woodbury, MN (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 21/18 (2006.01); C07C 45/58 (2006.01); C07C 17/26 (2006.01); C07C 17/093 (2006.01);
U.S. Cl.
CPC ...
C07C 45/58 (2013.01); C07C 17/093 (2013.01); C07C 17/26 (2013.01);
Abstract

A method of making α,ω-diiodoperfluoroalkanes includes combining: diatomic iodine, at least one perfluoroalkylene oxide represented by the formula wherein Rrepresents a perfluoroalkyl group; and at least one of: a) a first metallic compound comprising nickel, and a second metallic compound comprising molybdenum that is compositionally different from the first metallic compound; or b) a metallic alloy comprising from 50 to 70 percent by weight of nickel and from 20 to 40 percent by weight of molybdenum, based on the total weight of the metallic alloy, thereby producing at least one product represented by the formula I(CF)I, wherein n independently represents an integer in the range of from 1 to 11. The total weight of the at least one product wherein n is 3 or greater exceeds the total weight of the at least one product wherein n is 1 or 2 by a factor of at least 4.


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