The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 17, 2015

Filed:

Jan. 17, 2008
Applicants:

Xiangmin LI, Glen Mills, PA (US);

Lawrence M. Candela, Havertown, PA (US);

Mark A. Liepa, Exton, PA (US);

Inventors:

Xiangmin Li, Glen Mills, PA (US);

Lawrence M. Candela, Havertown, PA (US);

Mark A. Liepa, Exton, PA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 41/03 (2006.01); C07C 43/13 (2006.01); C07C 41/44 (2006.01);
U.S. Cl.
CPC ...
C07C 41/03 (2013.01); C07C 41/44 (2013.01);
Abstract

The invention is a process for producing a propylene glycol monoalkyl ether which comprises first reacting propylene oxide and an alcohol in the presence of an alkali or alkaline earth metal alkoxide catalyst to produce an alkoxylation mixture comprising propylene glycol monoalkyl ether; distilling the alkoxylation mixture to produce a first overhead stream comprising propylene oxide and alcohol and a first bottoms stream comprising propylene glycol monoalkyl ether; and then distilling the first bottoms stream to produce purified propylene glycol monoalkyl ether as a second overhead stream. The reaction and/or one or more of the distillation steps occur in the presence of an alkali metal borohydride. The process produces propylene glycol monoalkyl ether with low UV absorbance and reduced carbonyl impurities.


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