The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 10, 2015

Filed:

Jun. 18, 2013
Applicant:

David A. Kidwell, Alexandria, VA (US);

Inventor:

David A. Kidwell, Alexandria, VA (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01F 3/06 (2006.01); G01N 25/48 (2006.01); B01J 21/04 (2006.01); B01J 23/42 (2006.01); B01J 23/44 (2006.01); B01J 23/63 (2006.01); B01J 29/04 (2006.01);
U.S. Cl.
CPC ...
G01N 25/48 (2013.01); B01J 21/04 (2013.01); B01J 23/42 (2013.01); B01J 23/44 (2013.01); B01J 23/63 (2013.01); B01J 29/04 (2013.01);
Abstract

A method for producing excess enthalpy by impregnating metallic precursors on an oxide support that reduces sintering and particle growth; drying the impregnated support at a temperature where the particle growth is minimal; reducing the metallic precursors at a second temperature where the particle growth results in supported metallic particles 2 nm or less in size; and pressurizing the supported metallic particles in the presence of deuterium. The metal particles may comprise palladium, platinum, mixtures thereof, or mixtures of palladium and/or platinum with other elements. Also disclosed is a method for measuring excess enthalpy by placing a test material in a pressure vessel; heating the pressure vessel; evacuating the pressure vessel; introducing deuterium, hydrogen, or both into the pressure vessel; measuring the enthalpy generated during pressurization; again evacuating the pressure vessel; and measuring the enthalpy used during depressurization.


Find Patent Forward Citations

Loading…