The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 03, 2015

Filed:

Sep. 24, 2009
Applicants:

Tewodros Asefa, Somerset, NJ (US);

Yan-li Shi, Syracuse, NY (US);

Inventors:

Tewodros Asefa, Somerset, NJ (US);

Yan-Li Shi, Syracuse, NY (US);

Assignee:

Syracuse University, Syracuse, NY (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 33/58 (2006.01); B81C 99/00 (2010.01); G01N 33/543 (2006.01); B01J 21/08 (2006.01);
U.S. Cl.
CPC ...
G01N 33/587 (2013.01); B81C 99/0095 (2013.01); G01N 33/54353 (2013.01); B01J 21/08 (2013.01);
Abstract

A method of synthesizing corrugated and nanoporous microspheres including the steps of synthesizing substantially smooth spherical microspheres, and controlled wet-etching of the substantially smooth spherical microspheres with a basic solution having a pH above 10.00 is provided. The microspheres can include, for example, silica microspheres or titania microspheres of various sized diameters of between 50 nm and 600 nm. The basic solution can include an aqueous potassium cyanide solution or an aqueous potassium hydroxide solution. Methods of using the corrugated and nanoporous microspheres described herein are also provided.


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