The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 03, 2015

Filed:

Oct. 17, 2014
Applicants:

E3tec Service, Llc, Clarksville, MD (US);

Board of Trustees of Michigan State University, East Lansing, MI (US);

Inventors:

Chandrakant B. Panchal, Clarksville, MD (US);

John C. Prindle, Baton Rouge, LA (US);

Aspi Kolah, Mason, MI (US);

Dennis J. Miller, Okemos, MI (US);

Carl T. Lira, East Lansing, MI (US);

Assignees:

E3TEC Service, LLC, Clarksville, MD (US);

Board of Trustees of Michigan State University, East Lansing, MI (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/08 (2006.01); B01D 3/00 (2006.01);
U.S. Cl.
CPC ...
C07C 67/08 (2013.01); B01D 3/009 (2013.01);
Abstract

An integrated process and system for synthesis of organic-acid esters is provided. The method of synthesizing combines reaction and distillation where an organic acid and alcohol composition are passed through a distillation chamber having a plurality of zones. Side reactors are used for drawing off portions of the composition and then recycling them to the distillation column for further purification. Water is removed from a pre-reactor prior to insertion into the distillation column. An integrated heat integration system is contained within the distillation column for further purification and optimizing efficiency in the obtaining of the final product.


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