The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 06, 2015

Filed:

Aug. 07, 2013
Applicants:

Jian Zhi HU, Richland, WA (US);

Mary Y. HU, Richland, WA (US);

Mark R. Townsend, Kennewick, WA (US);

Johannes A. Lercher, Ottobrunn, DE;

Charles H. F. Peden, West Richland, WA (US);

Inventors:

Jian Zhi Hu, Richland, WA (US);

Mary Y. Hu, Richland, WA (US);

Mark R. Townsend, Kennewick, WA (US);

Johannes A. Lercher, Ottobrunn, DE;

Charles H. F. Peden, West Richland, WA (US);

Assignee:

BATTELLE MEMORIAL INSTITUTE, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01R 33/30 (2006.01); B23G 1/02 (2006.01); G01R 3/00 (2006.01);
U.S. Cl.
CPC ...
G01R 33/305 (2013.01); B23G 1/02 (2013.01); G01R 3/00 (2013.01); G01R 33/307 (2013.01); Y10T 29/49996 (2015.01); Y10T 409/300112 (2015.01);
Abstract

Re-usable ceramic magic angle spinning (MAS) NMR rotors constructed of high-mechanic strength ceramics are detailed that include a sample compartment that maintains high pressures up to at least about 200 atmospheres (atm) and high temperatures up to about least about 300° C. during operation. The rotor designs minimize pressure losses stemming from penetration over an extended period of time. The present invention makes possible a variety of in-situ high pressure, high temperature MAS NMR experiments not previously achieved in the prior art.


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