The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 06, 2015

Filed:

Oct. 15, 2012
Applicant:

Council of Scientific & Industrial Research, New Delhi, IN;

Inventors:

Amol Arvind Kulkarni, Maharashtra, IN;

Ramesh Anna Joshi, Maharashtra, IN;

Rohini Ramesh Joshi, Maharashtra, IN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 209/00 (2006.01); C07C 221/00 (2006.01); C07C 201/08 (2006.01);
U.S. Cl.
CPC ...
C07C 221/00 (2013.01); C07C 201/08 (2013.01);
Abstract

Disclosed herein is a continuous tubular reactor based conversion of acetophenones to amino substituted acetophenones wherein the nitration is carried out at −10 to 10° C. followed by reduction to m-nitrophenone resulting in uniform output of product, said process comprising the steps of: a) Nitrating acetophenone with nitrating agent (nitration mixture or fuming nitric acid) at −10 to 10° C.; b) Isolating m-nitro acetophenone from a mixture of o and m-nitro acetophenone and c) Reducing the m-nitro to obtain m-amino acetophenone.


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