The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 9127022 B1

PDF
Full Text
Expired
Date of Patent:
Sep. 08, 2015

Filed:

Dec. 14, 2014
Applicant:

Wuhan Kaidi Engineering Technology Research Institute Co., Ltd., Wuhan, CN;

Inventors:

Leiming Tao, Wuhan, CN;

Yilong Chen, Wuhan, CN;

Yanfeng Zhang, Wuhan, CN;

Yongjie Xue, Wuhan, CN;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01B 33/023 (2006.01); C07F 7/02 (2006.01);
U.S. Cl.
CPC ...
C07F 7/025 (2013.01);
Abstract

A method for preparing surface-modified nano silicon dioxide from rice hulls. The method includes: 1) pretreating rice hulls using a treating gas containing COto remove metal ions, impurities, and dusts, and desiccating and grinding the rice hulls; 2) submerging the rice hulls into a dilute solution of phosphoric acid, boric acid, hydrochloric acid, formic acid, acetic acid, propionic acid, butyric acid, or a strong-acid-weak-base salt for between 4 and 8 hrs, controlling the immersion temperature not to exceed 10° C., leaching a resulting mixture, removing a filtrate, and desiccating the rice hulls; and 3) calcining the rice hulls in the absence of oxygen at a temperature of between 300 and 450° C.


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