The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 08, 2015

Filed:

May. 13, 2013
Applicant:

Evonik Industries Ag, Essen, DE;

Inventors:

Martin Bindl, Ludwigshafen, DE;

Roland Herrmann, Maintal, DE;

Gunter Knaup, Bruchkobel, DE;

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C 231/02 (2006.01); C11D 3/32 (2006.01); C11D 7/32 (2006.01); C11D 17/00 (2006.01); C07C 227/18 (2006.01);
U.S. Cl.
CPC ...
C07C 231/02 (2013.01); C07C 227/18 (2013.01); C11D 3/32 (2013.01); C11D 7/3263 (2013.01); C11D 17/003 (2013.01); C07C 2101/14 (2013.01);
Abstract

The invention relates to a method for the synthesis of a compound according to formula I comprising the following steps: a) reacting a Dane salt according to formula II and a Dane salt according to formula III with a coupling reagent; b) adding a diamine according to formula IV to the reaction mixture; and c) adding an acid to the reaction mixture to adjust the pH value of the reaction to <7; wherein L represents a C-Calkyl group, a C-Caryl group, or a C-Calkylaryl group; Rand Rcan be identical or different and represent a hydrogen atom, a C-Calkyl group, a C-Chydroxyalkyl group, a C-Cthioether group, a C-Caryl group, a C-Calkylaryl group, a C-Calkylhydroxyaryl group, a C-Calkylheteroaryl group with 1 to 4 heteroatoms; or a C-Calkylcarboxylic moiety, which may be an acid, an amide, or which may be esterified with a C-Calkyl group or a C-Calkylaryl group; Rrepresents a C-Calkyl group; Rrepresents a hydrogen atom, or a C-Calkyl group; Rrepresents a C-Calkyl group; and X represents an alkali metal.


Find Patent Forward Citations

Loading…