The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 28, 2015

Filed:

Mar. 14, 2013
Applicant:

Honeywell International Inc., Morristown, NJ (US);

Inventors:

Haiyou Wang, Amherst, NY (US);

Huseh Sung Tung, Getzville, NY (US);

Selma Bektesevic, Williamsville, NY (US);

Assignee:

Honeywell International Inc., Morristown, NJ (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 17/25 (2006.01); C07C 17/38 (2006.01); C07C 17/383 (2006.01); C07C 17/42 (2006.01); C07C 21/04 (2006.01); C07C 17/278 (2006.01); C07C 17/386 (2006.01);
U.S. Cl.
CPC ...
C07C 17/42 (2013.01); C07C 17/278 (2013.01); C07C 17/38 (2013.01); C07C 17/386 (2013.01); C07C 17/25 (2013.01); C07C 21/04 (2013.01);
Abstract

This invention is directed to a method for mitigating HCl generation during 1230xa purification, which comprises the steps of; (a) adding a chelating agent into 1230xa crude, and (b) conducting the 1230xa purification in the presence of said chelating agent at a quantity sufficient to reduce or prevent 1230xa decomposition. Examples of chelating agent include tributyl phosphate (TBP), tripropyl phosphate (TPP), and triethyl phosphate (TEP). The concentration of chelating agent in 1230xa crude can range from 0.001 to 20 wt %, preferably from 0.01 to 10 wt %, and more preferably from 0.1 to 5 wt %.


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