The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 21, 2015

Filed:

Oct. 06, 2009
Applicants:

Michael Hill, Cologne, DE;

Mathias Dietz, Simmerath, DE;

Werner Krause, Huerth, DE;

Martin Sicken, Cologne, DE;

Inventors:

Michael Hill, Cologne, DE;

Mathias Dietz, Simmerath, DE;

Werner Krause, Huerth, DE;

Martin Sicken, Cologne, DE;

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07F 9/32 (2006.01); C09K 21/12 (2006.01); C07F 9/30 (2006.01); C08K 5/5313 (2006.01);
U.S. Cl.
CPC ...
C09K 21/12 (2013.01); C07F 9/301 (2013.01); C07F 9/3211 (2013.01); C08K 5/5313 (2013.01);
Abstract

A process for preparing mono-carboxy-functionalized dialkylphosphinic acids, dialkylphosphinic esters and dialkylphosphinic salts by means of alkylene oxides, characterized in that a) a phosphinic acid source (I) is reacted with olefins (IV) in the presence of a catalyst A to form an alkylphosphonous acid, its salt or ester (II), b) the resultant alkylphosphonous acid, its salt or ester (II) is reacted with alkylene oxides of the formula (V) in the presence of a catalyst B, to give a mono-functionalized dialkylphosphinic acid derivative (VI), and c) the resultant mono-functionalized dialkylphosphinic acid derivative (VI) is reacted in the presence of a catalyst C to give the mono-carboxy-functionalized dialkylphosphinic acid derivative (III), and the catalysts A and C are transition metals and/or transition-metal compounds and/or catalyst systems which are composed of a transition metal and/or a transition-metal compound and at least one ligand, and the catalyst B is a Lewis acid.


Find Patent Forward Citations

Loading…