The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 30, 2015

Filed:

Feb. 11, 2010
Applicants:

Wensheng Yang, Changchun, CN;

Jinglun Liang, Changchun, CN;

Jun LI, Changchun, CN;

Inventors:

Wensheng Yang, Changchun, CN;

Jinglun Liang, Changchun, CN;

Jun Li, Changchun, CN;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C09K 11/06 (2006.01); C01B 33/12 (2006.01); C09C 3/10 (2006.01); C09C 1/30 (2006.01); C09K 11/02 (2006.01); C01B 33/18 (2006.01); B82Y 30/00 (2011.01);
U.S. Cl.
CPC ...
C09C 1/30 (2013.01); C09K 11/02 (2013.01); C09K 11/06 (2013.01); C09K 2211/1096 (2013.01); C01B 33/18 (2013.01); C01P 2004/04 (2013.01); C01P 2004/34 (2013.01); C01P 2004/51 (2013.01); C01P 2004/52 (2013.01); C01P 2004/84 (2013.01); C01P 2004/64 (2013.01); B82Y 30/00 (2013.01);
Abstract

Provided are silica nanoparticles doped with dyes having a negative charge by using cationic polyelectrolyte as templet and preparing method thereof. The nanoparticles have a core-shell structure, inner core comprises cationic polyelectrolyte aggregates, in which fluorescent dye having a negative charge and SiO2 are doped, and optional additive having a negative charge, the shell is consisted of SiO2, wherein the sum of negative charge carried by the additives and the fluorescent dye is less than that of positive charge carried by the polyelectrolyte aggregates. The preparing method comprises the following steps: preparing complex solution of polyelectrolyte and fluorescent dye; prehydrolysis of organosilicon source; coating with organosilicon source. The method can be applied to dope silica with various fluorescent dyes having a negative charge. Various dyes can be doped at the same time, the doping amount, and particle diameter and shape of the product can be controlled by the method. The nanoparticles are spherical, the particle diameter thereof is uniform, and colloid formed therefrom is stable.


Find Patent Forward Citations

Loading…