The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 30, 2015

Filed:

Dec. 31, 2013
Applicant:

Scientific Design Company, Inc., Little Ferry, NJ (US);

Inventor:

Serguei Pak, Teaneck, NJ (US);

Assignee:

Scientific Design Company, Inc., Little Ferry, NJ (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 21/00 (2006.01); B01J 21/04 (2006.01); B01J 20/00 (2006.01); B01J 23/00 (2006.01); B01J 23/02 (2006.01); B01J 23/08 (2006.01); B01J 23/40 (2006.01); B01J 23/42 (2006.01); B01J 23/48 (2006.01); B01J 23/68 (2006.01);
U.S. Cl.
CPC ...
B01J 23/688 (2013.01);
Abstract

A method for producing a catalyst effective in the oxidative conversion of ethylene to ethylene oxide, the method comprising subjecting a refractory carrier impregnated with a liquid silver-containing solution to a calcination process, wherein the calcination process comprises a solvent removal step in which the silver-impregnated carrier is heated to a base temperature (T) of at least 80° C. and up to about 200° C. to produce a dry carrier impregnated with ionic silver, followed by a silver reduction step in which the dry carrier is gradually heated above the base temperature to a maximum temperature (T) of at least 350° C. and up to about 500° C. and then gradually cooled to the base temperature, wherein the method is conducted such that (T−T)×HW is at least 2000 min.° C. wherein HW is a full width at half maximum of a temperature versus time curve delineated by the silver reduction step.


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