The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 9067188 B1

PDF
Full Text
Expired
Date of Patent:
Jun. 30, 2015

Filed:

Dec. 20, 2012
Applicant:

Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, CN;

Inventors:

Jing Chen, Lanzhou, CN;

Heyuan Song, Lanzhou, CN;

Chungu Xia, Lanzhou, CN;

Meirong Kang, Lanzhou, CN;

Ronghua Jin, Lanzhou, CN;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C 41/50 (2006.01); C07C 41/56 (2006.01); C07C 41/60 (2006.01); B01J 19/00 (2006.01); B01J 19/24 (2006.01); B01J 14/00 (2006.01); C07C 41/58 (2006.01);
U.S. Cl.
CPC ...
B01J 14/00 (2013.01); B01J 19/2465 (2013.01); B01J 19/00 (2013.01); C07C 41/60 (2013.01); C07C 41/56 (2013.01); C07C 41/50 (2013.01); C07C 41/58 (2013.01);
Abstract

A reaction system and method for producing polyoxymethylene dialkyl ethers (RO(CHO)R, n=1-8) by continuous acetalation of formaldehyde and aliphatic alcohol in the presence of an acid ionic liquid catalyst. The reaction system includes an acetalation reaction unit, a product separation unit, and a catalyst regeneration unit. The recyclable material and catalyst are separated by combining extraction and rectification, and a recovery rate of more than 99% for the catalyst is achieved. Water, as the byproduct, is separated from the reaction system by destroying the azeotrope of water, alcohol, aldehyde, and RO(CHO)R, so that the product separation and catalyst regeneration are facilitated and the catalytic cycle is achieved.


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Chen, Jing. (2015). System and method for continuously producing polyoxymethylene dialkyl ethers (U.S. Patent No. 9067188). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/9067188

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