The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 02, 2015

Filed:

Apr. 01, 2011
Applicants:

Michael H. Gelb, Seattle, WA (US);

Frantisek Turecek, Seattle, WA (US);

James Bollinger, Seattle, WA (US);

Inventors:

Michael H. Gelb, Seattle, WA (US);

Frantisek Turecek, Seattle, WA (US);

James Bollinger, Seattle, WA (US);

Assignee:

University of Washington, Seattle, WA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D 211/70 (2006.01); C07D 211/82 (2006.01); C07D 213/00 (2006.01); C07D 211/92 (2006.01); C07D 213/18 (2006.01); C07D 213/20 (2006.01); G01N 33/88 (2006.01); G01N 33/92 (2006.01); H01J 49/16 (2006.01);
U.S. Cl.
CPC ...
C07D 213/20 (2013.01); G01N 33/88 (2013.01); G01N 33/92 (2013.01); H01J 49/165 (2013.01);
Abstract

Method and reagent for converting a carboxylic acid to a positively charge amide are described. The method and reagent facilitate positive ion mass spectral analysis of carboxylic acids. The method includes reacting a carboxylic acid with a compound having formula I: wherein A and B are aromatic rings, ring A includes a quaternized nitrogen and has n additional ring atoms, each additional ring atom optionally substituted with an Rgroup, and n is an integer from 4 to 10, and ring B includes a carbon atom and has m additional ring atoms, each additional ring atom optionally substituted with an Rgroup, and m is an integer from 4 to 10. The compound includes at least one Ror Rgroup, and the at least one Rand Rgroup is -L-N(Z)H; and Xis a counterion.


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