The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 9045399 B1

PDF
Full Text
Expired
Date of Patent:
Jun. 02, 2015

Filed:

Mar. 02, 2011
Applicants:

Shinobu Maruno, Niihama, JP;

Koichi Nakazawa, Tsukuba, JP;

Inventors:

Shinobu Maruno, Niihama, JP;

Koichi Nakazawa, Tsukuba, JP;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 309/66 (2006.01); C07C 303/28 (2006.01); C07C 303/44 (2006.01);
U.S. Cl.
CPC ...
C07C 303/28 (2013.01); C07C 303/44 (2013.01);
Abstract

An aromatic organic solvent solution of a methanesulfonic acid alkyl ester having high thermal stability is obtained by reacting an alkyl alcohol with methanesulfonyl chloride in an aromatic organic solvent in the presence of a tertiary amine, and washing the resulting aromatic organic solvent solution of a crude methanesulfonic acid alkyl ester with an aqueous alkali metal carbonate solution. The washing is performed using the aqueous alkali metal carbonate solution having a concentration of 1 to 3 mass % in an amount of 4 to 6 parts by mass per 1 part by mass of the alkyl alcohol.


Find Patent Forward Citations

Maruno, Shinobu. (2015). Method for producing methanesulfonic acid alkyl ester solution (U.S. Patent No. 9045399). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/9045399

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