The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 24, 2015

Filed:

Jun. 20, 2011
Applicants:

Chungu Xia, Gansu, CN;

Heyuan Song, Gansu, CN;

Jing Chen, Gansu, CN;

Zhen LI, Gansu, CN;

Inventors:

Chungu Xia, Gansu, CN;

Heyuan Song, Gansu, CN;

Jing Chen, Gansu, CN;

Zhen Li, Gansu, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 41/14 (2006.01); C07C 41/56 (2006.01); C07C 41/58 (2006.01);
U.S. Cl.
CPC ...
C07C 41/56 (2013.01); C07C 41/58 (2013.01);
Abstract

It is disclosed a method for preparing polyoxymethylene dimethyl ethers by continuous polymerization and acetalation reactions. The method may include two steps: performing a polymerization reaction of an aqueous formaldehyde solution under catalysis of an ionic liquid IL I to obtain a mixed aqueous solution of trioxymethylene and formaldehyde; and an acetalation reaction of the mixed aqueous solution of trioxymethylene and formaldehyde with methanol is performed under catalysis of an ionic liquid IL II to prepare polyoxymethylene dimethyl ethers. The method may use an aqueous formaldehyde solution as a starting material to prepare polyoxymethylene dimethyl ethers by continuous polymerization and acetalation reactions, achieving a high use ratio of formaldehyde. A film evaporator is used in the invention, realizing a rapid separation and recycling of the light components, with a high separation efficiency. The separation of the catalyst is simple, thereby realizing recycling of the catalyst.


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Xia, Chungu. (2015). Method for preparing polyoxymethylene dimethyl ethers by acetalation reaction of formaldehyde with methanol (U.S. Patent No. 8987521). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/8987521

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