The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 10, 2015

Filed:

May. 25, 2010
Applicants:

Beihai MA, Naperville, IL (US);

Manoj Narayanan, Woodridge, IL (US);

Stephen E. Dorris, LaGrange Park, IL (US);

Uthamalingam Balachandran, Willowbrook, IL (US);

Inventors:

Beihai Ma, Naperville, IL (US);

Manoj Narayanan, Woodridge, IL (US);

Stephen E. Dorris, LaGrange Park, IL (US);

Uthamalingam Balachandran, Willowbrook, IL (US);

Assignee:

UChicago Argonne, LLC, Chicago, IL (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B05D 7/00 (2006.01); C23C 26/00 (2006.01); C04B 35/491 (2006.01); C04B 35/624 (2006.01); C23C 18/12 (2006.01); H01G 4/12 (2006.01);
U.S. Cl.
CPC ...
C23C 26/00 (2013.01); C04B 35/491 (2013.01); C04B 35/624 (2013.01); C23C 18/1208 (2013.01); C23C 18/1225 (2013.01); C23C 18/1241 (2013.01); C23C 18/1254 (2013.01); C23C 18/1283 (2013.01); H01G 4/1218 (2013.01); H01G 4/1245 (2013.01); C04B 2235/3227 (2013.01); C04B 2235/3232 (2013.01); C04B 2235/3244 (2013.01); C04B 2235/3296 (2013.01); C04B 2235/441 (2013.01); C04B 2235/443 (2013.01); C04B 2235/449 (2013.01); C04B 2235/6562 (2013.01); C04B 2235/6565 (2013.01); C04B 2235/6584 (2013.01); C04B 2235/768 (2013.01);
Abstract

The present invention provides a method for fabricating a ceramic film on a copper foil. The method comprises applying a layer of a sol-gel composition onto a copper foil. The sol-gel composition comprises a precursor of a ceramic material suspended in 2-methoxyethanol. The layer of sol-gel is then dried at a temperature up to about 250° C. The dried layer is then pyrolyzed at a temperature in the range of about 300 to about 450° C. to form a ceramic film from the ceramic precursor. The ceramic film is then crystallized at a temperature in the range of about 600 to about 750° C. The drying, pyrolyzing and crystallizing are performed under a flowing stream of an inert gas. In some embodiments an additional layer of the sol-gel composition is applied onto the ceramic film and the drying, pyrolyzing and crystallizing steps are repeated for the additional layer to build up a thicker ceramic layer on the copper foil. The process can be repeated one or more times if desired.


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