The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 09, 2014

Filed:

Mar. 26, 2012
Applicant:

Tetsuo Yokoyama, Hyogo, JP;

Inventor:

Tetsuo Yokoyama, Hyogo, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G01N 30/02 (2006.01); G01N 21/64 (2006.01); G01N 30/30 (2006.01); G01N 30/74 (2006.01); G01N 30/84 (2006.01); G01N 30/88 (2006.01);
U.S. Cl.
CPC ...
G01N 21/6486 (2013.01); G01N 30/30 (2013.01); G01N 2030/3007 (2013.01); G01N 30/74 (2013.01); G01N 2030/8435 (2013.01); G01N 2030/8836 (2013.01); G01N 30/88 (2013.01); G01N 30/84 (2013.01);
Abstract

Disclosed are an apparatus and method for separation analysis of mannose-6-phosphate (M6P) by post-column fluorescence detection method. The apparatus is based on chromatography, and includes a column with a solid phase having affinity for phosphate, a flow path for the eluate, a heater installed on the flow path for M6P and a basic amino acid to react by heating the eluate in the flow path, and a fluorescence detector installed downstream of the heater for continuously irradiating the eluate with excitation light and measuring the intensity of the emission, and may include in the flow path a supply channel for addition of a basic amino acid between the column and the heater. The method is characterized in that it uses the apparatus and a second mobile phase consisting of a second buffer containing phosphate of predetermined concentration and adjusted to a predetermined pH.


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