The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 11, 2014

Filed:

Dec. 26, 2007
Applicants:

Aruna Zhamu, Centerville, OH (US);

Jiusheng Guo, Centerville, OH (US);

Bor Z. Jang, Centerville, OH (US);

Inventors:

Aruna Zhamu, Centerville, OH (US);

Jiusheng Guo, Centerville, OH (US);

Bor Z. Jang, Centerville, OH (US);

Assignee:

Nanotek Instruments, Inc., Dayton, OH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 31/04 (2006.01); C09C 1/56 (2006.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01); C09C 1/44 (2006.01); C09C 1/46 (2006.01);
U.S. Cl.
CPC ...
C01B 31/0469 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01); C01B 31/0415 (2013.01); C09C 1/44 (2013.01); C09C 1/46 (2013.01); C09C 1/565 (2013.01); C01B 2204/04 (2013.01); C01B 2204/32 (2013.01); C01P 2004/03 (2013.01); C01P 2004/32 (2013.01);
Abstract

A method of producing nano-scaled graphene platelets (NGPs) having an average thickness no greater than 50 nm, typically less than 2 nm, and, in many cases, no greater than 1 nm. The method comprises (a) intercalating a supply of meso-carbon microbeads (MCMBs) to produce intercalated MCMBs; and (b) exfoliating the intercalated MCMBs at a temperature and a pressure for a sufficient period of time to produce the desired NGPs. Optionally, the exfoliated product may be subjected to a mechanical shearing treatment, such as air milling, air jet milling, ball milling, pressurized fluid milling, rotating-blade grinding, or ultrasonicating. The NGPs are excellent reinforcement fillers for a range of matrix materials to produce nanocomposites. Nano-scaled graphene platelets are much lower-cost alternatives to carbon nano-tubes or carbon nano-fibers.


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