The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 04, 2014

Filed:

Dec. 16, 2011
Applicants:

Eric H. Jordan, Storrs, CT (US);

Steven L. Suib, Storrs, CT (US);

Aparna Iyer, Storrs, CT (US);

Jacquelynn Garofano, Milford, CT (US);

Chun-hu Chen, Pingtung, TW;

Inventors:

Eric H. Jordan, Storrs, CT (US);

Steven L. Suib, Storrs, CT (US);

Aparna Iyer, Storrs, CT (US);

Jacquelynn Garofano, Milford, CT (US);

Chun-Hu Chen, Pingtung, TW;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B28B 1/00 (2006.01); B28B 3/00 (2006.01); C04B 33/32 (2006.01); C04B 33/36 (2006.01); C01B 33/12 (2006.01); C01F 5/06 (2006.01); C01F 17/00 (2006.01); B82Y 30/00 (2011.01); C04B 35/505 (2006.01); C04B 35/626 (2006.01); B82Y 40/00 (2011.01); C01B 13/18 (2006.01); C04B 35/624 (2006.01); C01F 7/16 (2006.01); C04B 35/053 (2006.01); C04B 35/645 (2006.01); C04B 35/632 (2006.01); C04B 35/636 (2006.01);
U.S. Cl.
CPC ...
C01B 13/185 (2013.01); C01F 5/06 (2013.01); C01F 17/0043 (2013.01); C04B 2235/9653 (2013.01); C04B 2235/3225 (2013.01); C01P 2002/72 (2013.01); B82Y 30/00 (2013.01); C04B 35/505 (2013.01); C04B 35/6267 (2013.01); C04B 2235/3206 (2013.01); B82Y 40/00 (2013.01); C01P 2004/64 (2013.01); C04B 35/624 (2013.01); C01F 7/162 (2013.01); C04B 2235/80 (2013.01); C04B 35/053 (2013.01); C04B 35/62675 (2013.01); C04B 35/645 (2013.01); C04B 2235/3244 (2013.01); C04B 2235/447 (2013.01); C04B 35/632 (2013.01); C04B 35/636 (2013.01); C01P 2004/04 (2013.01); C01B 13/18 (2013.01);
Abstract

Nanocomposites of multi-phase metal oxide ceramics have been produced from water soluble salts of the resulting metal oxides by a foaming esterification sol-gel method. The evolution of volatile gases at elevated temperature during the esterification reaction causes the formation of a foam product. Nanocomposites of multi-phase metal oxide ceramics have also been produced by a cation polymer precursor method. In this second method, the metal cations are chelated by the polymer and the resulting product is gelled and foamed. Calcination of the resulting foams gives nanocomposite powders with extremely fine, uniform grains and phase domains. These microstructures are remarkably stable both under post-calcination heat treatment and during consolidation by hot-pressing.


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