The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 28, 2014

Filed:

Oct. 28, 2010
Applicants:

John T. Vaughey, Elmhurst, IL (US);

Andrew Jansen, Bolingbrook, IL (US);

Christopher D. Joyce, Columbus, OH (US);

Inventors:

John T. Vaughey, Elmhurst, IL (US);

Andrew Jansen, Bolingbrook, IL (US);

Christopher D. Joyce, Columbus, OH (US);

Assignee:

Uchicago Argonne, LLC, Chicago, IL (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
H01M 4/90 (2006.01); H01M 4/485 (2010.01); H01M 4/587 (2010.01); C01G 23/047 (2006.01); H01M 10/0525 (2010.01); C07F 7/00 (2006.01);
U.S. Cl.
CPC ...
C01G 23/047 (2013.01); C01P 2002/88 (2013.01); H01M 4/485 (2013.01); H01M 4/587 (2013.01); H01M 10/0525 (2013.01); C07F 7/006 (2013.01); C01P 2006/40 (2013.01); C01P 2002/72 (2013.01); Y02E 60/122 (2013.01); C01P 2004/03 (2013.01);
Abstract

An isolated salt comprising a compound of formula (HX)(TiO(Y)) or a hydrate thereof, wherein X is 1,4-diazabicyclo[2.2.2]octane (DABCO), and Y is oxalate anion (CO), when heated in an oxygen-containing atmosphere at a temperature in the range of at least about 275° C. to less than about 400° C., decomposes to form an amorphous titania/carbon composite material comprising about 40 to about 50 percent by weight titania and about 50 to about 60 percent by weight of a carbonaceous material coating the titania. Heating the composite material at a temperature of about 400 to 500° C. crystallizes the titania component to anatase. The titania materials of the invention are useful as components of the anode of a lithium or lithium ion electrochemical cell.


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