The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 14, 2014

Filed:

Jun. 24, 2010
Applicants:

Kazuhiko Sakamoto, Himeji, JP;

Koji Ueno, Himeji, JP;

Yoshitake Ishii, Himeji, JP;

Masatsugu Kitaura, Himeji, JP;

Inventors:

Kazuhiko Sakamoto, Himeji, JP;

Koji Ueno, Himeji, JP;

Yoshitake Ishii, Himeji, JP;

Masatsugu Kitaura, Himeji, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/42 (2006.01); B01D 9/00 (2006.01); C07C 51/43 (2006.01);
U.S. Cl.
CPC ...
B01D 9/0013 (2013.01); C07C 51/43 (2013.01);
Abstract

A crystallization device and a crystallization process are provided for obtaining (meth)acrylic acid with higher purity without causing leakage of a crude solution by preventing complete clogging in a crystallization tube from occurring. The device for crystallizing (meth)acrylic acid includes a crude (meth)acrylic acid solution supply part, a crystallization tube, a heat medium supply tube, a heat medium discharge tube, a storage part of a crude (meth)acrylic acid solution passed through the crystallization tube, a tube for circulating and supplying the crude (meth)acrylic acid solution to the supply part from the storage part, and a pump for circulating and supplying the crude (meth)acrylic acid solution to the supply part from the storage part, and also includes a pressure meter in the circulate-supply tube. The device is used for carrying out dynamic crystallization in a batch manner by circulating the crude (meth)acrylic acid solution to flow the crude solution downward along the inner wall of the crystallization tube in a coating film-like state.


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