The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 30, 2014

Filed:

Aug. 07, 2013
Applicant:

Newron Pharmaceuticals S.p.a., Bresso, IT;

Inventors:

Elena Barbanti, Cologno Monzese, IT;

Laura Faravelli, Garbagnate Milanese, IT;

Patricia Salvati, Arese, IT;

Renato Canevotti, Chignolo d'Isola, IT;

Francesco Ponzini, Chignolo d'Isola, IT;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
A61K 31/165 (2006.01); C07C 231/12 (2006.01); C07C 233/09 (2006.01); A61K 31/198 (2006.01); C07C 231/24 (2006.01); C07C 251/24 (2006.01); A61K 31/197 (2006.01); A61K 45/06 (2006.01);
U.S. Cl.
CPC ...
C07C 251/24 (2013.01); A61K 31/198 (2013.01); C07C 231/12 (2013.01); C07C 231/24 (2013.01); A61K 31/197 (2013.01); A61K 31/165 (2013.01); A61K 45/06 (2013.01);
Abstract

A process for obtaining therapeutically active 2-[4-(3- and 2-(fluorobenzyloxy)benzylamino]propanamides, and their salts with pharmaceutically acceptable acids with high purity degree, in particular, with a content of dibenzyl derivatives impurities lower than 0.03%, preferably lower than 0.01% by weight. The process is carried out by submitting the Schiff bases intermediates 2-[4-(3- and 2-fluorobenzyloxy)benzylideneamino]propanamides to a reduction reaction with a reducing agent selected from sodium borohydride and potassium borohydride in an appropriate amount of an organic solvent selected from C-Clower alkanols, allowing the formation and presence during a substantial position of the reduction reaction course of a suspension of the Schiff base into the saturated solution of the Schiff base into the same organic solvent.


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