The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 09, 2014

Filed:

Jul. 07, 2010
Applicants:

Laurent Saint-jalmes, Vourles, FR;

Francois Metz, Irigny, FR;

Inventors:

Laurent Saint-Jalmes, Vourles, FR;

Francois Metz, Irigny, FR;

Assignee:

Rhodia Operations, Aubervilliers, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/58 (2006.01); C07C 53/18 (2006.01); C07C 51/64 (2006.01); C07C 51/04 (2006.01); C07C 51/62 (2006.01);
U.S. Cl.
CPC ...
C07C 51/58 (2013.01); C07C 51/64 (2013.01); C07C 51/04 (2013.01); C07C 51/62 (2013.01);
Abstract

The present invention relates to a method for preparing a halogenoacetyl fluoride and the derivatives thereof. The inventive method for preparing a halogenoacetyl fluoride acid is characterized in that said method includes: a step of preparing a halogenoacetyl halide by photo-oxidation of a halogenoethylene compound in conditions such that the transformation rate of the halogenoethylene compound into halogenoacetyl halide is no higher than 80%, producing a reaction mixture essentially including halogenoacetyl halide and the excess halogenoethylene compound; a step of partial fluorination of the mixture obtained by reacting the latter with hydrofluoric acid suitable for obtaining a mixture of halogenoacetyl fluoride and the excess halogenoethylene compound; a step of separating the halogenoacetyl fluoride and the excess halogenoethylene compound. The invention can be used, specifically, for preparing the trichloroacetyl fluoride used as an intermediate species in the production of trifluoroacetic acid.


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