The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 09, 2014

Filed:

Nov. 16, 2010
Applicants:

David M. Glaser, New Britain, CT (US);

Roderick Coffey, Middletown, CT (US);

John G. Woods, Iii, Farmington, CT (US);

Anthony F. Jacobine, Meriden, CT (US);

Inventors:

David M. Glaser, New Britain, CT (US);

Roderick Coffey, Middletown, CT (US);

John G. Woods, III, Farmington, CT (US);

Anthony F. Jacobine, Meriden, CT (US);

Assignee:

Henkel US IP LLC, Rocky Hill, CT (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08F 20/10 (2006.01); B01J 19/18 (2006.01); C08F 2/00 (2006.01); B01J 14/00 (2006.01); C08F 293/00 (2006.01); B01J 16/00 (2006.01); B01J 19/00 (2006.01); C08F 220/18 (2006.01);
U.S. Cl.
CPC ...
C08F 220/18 (2013.01); B01J 2219/002 (2013.01); B01J 2219/00069 (2013.01); B01J 19/1881 (2013.01); C08F 2/00 (2013.01); B01J 14/005 (2013.01); B01J 2219/00238 (2013.01); B01J 2219/00094 (2013.01); C08F 293/005 (2013.01); B01J 2219/00162 (2013.01); B01J 16/005 (2013.01); B01J 2219/00213 (2013.01); B01J 2219/00063 (2013.01); B01J 19/0066 (2013.01); B01J 2219/00231 (2013.01); C08F 2438/01 (2013.01);
Abstract

A method of conducting controlled radical polymerization, including: (a) providing a mixture of at least one monomer; at least one monomer solvent; at least one compound metal coordinating capable; and at least one initiator; (b) directing the mixture at a rate over a solid catalyst surface contained in an external chamber to the vessel, the catalyst including a metal or metal compound capable of at least two oxidation states; (c) monitoring the reaction vessel temperature; (d) adjusting the flow rate when the temperature is outside a selected temperature range; and (e) allowing the polymerization to proceed to desired conversion level.


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