The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 02, 2014

Filed:

May. 16, 2011
Applicants:

Tsuyoshi Ito, Hitachi, JP;

Hideyuki Hosokawa, Hitachinaka, JP;

Yukio Hirama, Mito, JP;

Makoto Nagase, Mito, JP;

Inventors:

Tsuyoshi Ito, Hitachi, JP;

Hideyuki Hosokawa, Hitachinaka, JP;

Yukio Hirama, Mito, JP;

Makoto Nagase, Mito, JP;

Assignee:
Attorney:
Int. Cl.
CPC ...
B05D 7/22 (2006.01); G21C 19/00 (2006.01); C23C 18/12 (2006.01);
U.S. Cl.
CPC ...
G21C 19/00 (2013.01); C23C 18/1283 (2013.01); C23C 18/1241 (2013.01); C23C 18/1216 (2013.01);
Abstract

Both ends of a circulation pipe of a film formation apparatus are connected to a piping of a BWR plant. A chemical including chromium ions and formic acid is injected into a film formation solution flowing in the circulation pipe heated to a temperature within a range from 60° C. to 100° C. Furthermore, a chemical including iron (II) ions and formic acid, hydrogen peroxide, and hydrazine are injected into the circulation pipe. Due to the injection of these chemicals, a film formation solution of pH 7.0 including iron (II) ions, chromium ions, formic acid, hydrogen peroxide, and hydrazine is generated in the circulation pipe. This film formation solution includes hydrazine of, for example, 1000 ppm. The film formation solution is supplied to the piping, thus, a Fe—CrOfilm (here, 0<X≦0.1) is formed on the inner surface of the piping. The above method of forming the ferrite film on a structural member (for example, the piping) can be shortened time required to form the ferrite film.


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