The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 24, 2014

Filed:

Sep. 06, 2012
Applicants:

R. Jay Warner, Houston, TX (US);

Melchoir Meilchen, Houston, TX (US);

Nathan Kirk Powell, Waxahachie, TX (US);

Inventors:

R. Jay Warner, Houston, TX (US);

Melchoir Meilchen, Houston, TX (US);

Nathan Kirk Powell, Waxahachie, TX (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/573 (2006.01); C07C 53/12 (2006.01);
U.S. Cl.
CPC ...
C07C 53/12 (2013.01);
Abstract

In one embodiment, the invention is to a process for purifying acetic anhydride. The process includes the steps of feeding a liquid crude acetic anhydride stream directly to a distillation column and separating the liquid crude acetic anhydride stream to produce a light ends stream, a sidedraw and a residue stream. The sidedraw comprises substantially pure acetic anhydride product. The distillation column is operated at a pressure less than 101 kPa. The substantially pure acetic anhydride product comprises greater than 98 wt. % acetic anhydride, has a permanganate time of greater than 10 minutes, and has an APHA color of less than 10.


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