The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 03, 2014

Filed:

Nov. 13, 2012
Applicant:

Lyondell Chemical Technology, L.p., Houston, TX (US);

Inventors:

Daniel F. White, Houston, TX (US);

Brian A. Salisbury, Beach City, TX (US);

Jenny M. Oran Osment, Humble, TX (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/141 (2006.01); C07C 29/16 (2006.01); C07C 29/44 (2006.01); C07C 29/48 (2006.01); C07C 31/20 (2006.01);
U.S. Cl.
CPC ...
C07C 29/16 (2013.01); C07C 29/44 (2013.01); C07C 29/48 (2013.01); C07C 31/207 (2013.01);
Abstract

Embodiments of the present disclosure include methods of effecting process control in a reaction system for the production of 1,4-butanediol, the method including determining at least one property of a sample from the reaction system using Raman spectroscopy, and adjusting at least one parameter of the reaction system in response to the at least one determined property. Embodiments may also include methods of producing 1,4-butanediol, the method including reacting allyl alcohol with carbon monoxide and hydrogen in the presence of a solvent and a catalyst to produce a reactor fluid, sampling the reaction, determining at least one property of the sample using Raman spectroscopy, and adjusting the reaction in response to the at least one determined property.


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