The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 21, 2014

Filed:

Nov. 25, 2008
Applicants:

Vincent Schanen, Lyons, FR;

Olivier Buisine, Saint Genis Laval, FR;

François Metz, Irigny, FR;

Bernard Besson, Les Echets, FR;

Inventors:

Vincent Schanen, Lyons, FR;

Olivier Buisine, Saint Genis Laval, FR;

François Metz, Irigny, FR;

Bernard Besson, Les Echets, FR;

Assignee:

Rhodia Operations, Aubervilliers, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 313/04 (2006.01);
U.S. Cl.
CPC ...
Abstract

The present invention relates to a method for preparing a highly pure trifluoromethanesulphinic acid. The method of the invention for preparing a highly pure trifluoromethanesulphinic acid, starting from an aqueous mixture comprising a trifluoromethanesulphinic acid salt, a trifluoroacetic acid salt and saline impurities resulting from the method for preparing same, is characterized in that said mixture is subjected to the following operations: —acidification such that the trifluoroacetic acid salt and the triflinic acid salt are released in an acid form, —separation of the trifluoroacetic acid and trifluoromethanesulphinic acid by distillation enabling the trifluoroacetic acid to be recovered at the top of the distillation and the trifluoromethanesulphinic acid to be recovered at the bottom of the distillation, —separation by distillation of the trifluoromethanesulphinic acid present in the distillation residue previously obtained.


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