The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 05, 2013

Filed:

Nov. 17, 2009
Applicants:

Stephen P. Velarde, Christiansburg, VA (US);

Andrew J. Sanderson, Blacksburg, VA (US);

Inventors:

Stephen P. Velarde, Christiansburg, VA (US);

Andrew J. Sanderson, Blacksburg, VA (US);

Assignee:

Alliant Techsystems Inc., Arlington, VA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/80 (2006.01); C07C 31/22 (2006.01);
U.S. Cl.
CPC ...
Abstract

Methods of purifying BT are disclosed. The method comprises adding at least one polyhydroxyl compound to a crude BT mixture comprising BT and at least one boron-containing compound to form a polyhydroxyl compound/BT mixture. In one embodiment, the polyhydroxyl compound/BT mixture is then heated to a temperature greater than the boiling point of BT but less than the boiling point of the at least one polyhydroxyl compound. In another embodiment, the polyhydroxyl compound/BT mixture is heated to a temperature greater than the melting point of the at least one polyhydroxyl compound, and then to a temperature greater than the boiling point of BT but less than the boiling point of the at least one polyhydroxyl compound. A composition comprising BT is also disclosed.


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