The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 8357796 B1

PDF
Full Text
Expired
Date of Patent:
Jan. 22, 2013

Filed:

Jan. 24, 2005
Applicants:

Yulin Ren, Athens, OH (US);

Klaus B. Himmeldirk, Vincent, OH (US);

Xiaozhou Chen, Athens, OH (US);

Inventors:

Yulin Ren, Athens, OH (US);

Klaus B. Himmeldirk, Vincent, OH (US);

Xiaozhou Chen, Athens, OH (US);

Assignee:

Ohio University, Athens, OH (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07H 1/06 (2006.01);
U.S. Cl.
CPC ...
Abstract

A simple, inexpensive, and efficient method for separation and purification of the α-and β-forms of penta-O-galloyl-D-glucose (PGG) without the need for HPLC. The methods provided herein are useful for separation α-PGG or β-PGG from a mixture containing α-PGG and β-PGG and other chemicals. The method for separation of α-PGG from a mixture of α-PGG and β-PGG comprises the steps of: adding water to a sample containing 50% or more α-PGG and 50% or less β-PGG; mixing the PGG and water to dissolve the PGG; filtering out any undissolved particles; and allowing the filtered solution to stand undisturbed until crystals form.


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