The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 25, 2012

Filed:

Sep. 01, 2011
Applicants:

Dan V. Goia, Potsdam, NY (US);

Marco Lopez, Frankfurt, DE;

Tapan Kumar Sau, Chandigarh, IN;

Mihaela-ortansa Jitianu, Potsdam, NY (US);

Inventors:

Dan V. Goia, Potsdam, NY (US);

Marco Lopez, Frankfurt, DE;

Tapan Kumar Sau, Chandigarh, IN;

Mihaela-Ortansa Jitianu, Potsdam, NY (US);

Assignee:

Umicore AG & Co. KG, Hanau-Wolfgang, DE;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/00 (2006.01); B01J 23/40 (2006.01); B01J 23/42 (2006.01); B01J 23/44 (2006.01); B01J 21/18 (2006.01); H01M 4/02 (2006.01); H01M 4/36 (2006.01); H01M 4/90 (2006.01); H01M 4/92 (2006.01); H01M 4/94 (2006.01);
U.S. Cl.
CPC ...
Abstract

The invention provides a method for manufacturing supported noble metal based alloy catalysts with a high degree of alloying and a small crystallite size. The method involves using polyol solvents as reaction medium and comprises a two-step reduction process in the presence of a support material. In the first step, the first metal (transition metal; e.g. Co, Cr, Ru) is activated by increasing the reaction temperature to 80 to 160° C. In the second step, the second metal (noble metal; e.g. Pt, Pd, Au) is added and the slurry is heated to the boiling point of the polyol solvent in a range of 160 to 300 ° C. The catalysts manufactured according to the method are used as electrocatalysts for polymer electrolyte membrane fuel cells (PEMFC), direct-methanol fuel cells (DMFC) or as gas phase catalysts for CO oxidation or exhaust gas purification.


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