The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 07, 2012

Filed:

Apr. 08, 2010
Applicants:

Wei Liu, Richland, WA (US);

John E. Holladay, Kennewick, WA (US);

Feng Zheng, Richland, WA (US);

Heather M. Brown, Kennewick, WA (US);

Alan R. Cooper, Richland, WA (US);

Inventors:

Wei Liu, Richland, WA (US);

John E. Holladay, Kennewick, WA (US);

Feng Zheng, Richland, WA (US);

Heather M. Brown, Kennewick, WA (US);

Alan R. Cooper, Richland, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 307/42 (2006.01); C07D 307/45 (2006.01); C07D 493/04 (2006.01);
U.S. Cl.
CPC ...
Abstract

Presently disclosed are methods and apparatus for separation of reaction products from reaction mixtures in an ionic liquid catalysis process, particularly in conversion of biomass, cellulose, and sugars into chemical intermediates such as 5-hydroxymethylfurfural (HMF). In one embodiment an ion exclusion adsorption mechanism is used for the separation process. The process comprises (i) mixing the ionic liquid-containing reaction mixture with de-ionized water, (ii) flowing the water solution mixture into an adsorption column, (iii) eluting the column with a water- and/or alcohol-based fluid, and (iv) collecting separated fractions at different elution times.


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