The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 27, 2012

Filed:

Jan. 09, 2009
Applicants:

Yuuki Matsuda, Osaka, JP;

Kazuyoshi Ichihara, Osaka, JP;

Takeomi Hirasaka, Osaka, JP;

Takuya Ichida, Osaka, JP;

Inventors:

Yuuki Matsuda, Osaka, JP;

Kazuyoshi Ichihara, Osaka, JP;

Takeomi Hirasaka, Osaka, JP;

Takuya Ichida, Osaka, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/10 (2006.01); C07C 31/34 (2006.01);
U.S. Cl.
CPC ...
Abstract

There is provided a method for separating and collecting at least alcohol with a high purity from an azeotropic mixture of olefin and alcohol. The method conducts the following steps: an azeotropic mixture crystallization step of subjecting an azeotropic mixture of alcohol and olefin represented by the formula: RfCH═CH[wherein Rf represents a linear perfluoroalkyl group having 1 to 10 carbon atoms] to a crystallization procedure to separate the mixture into an olefin portion having a higher olefin concentration than that of the original azeotropic mixture and an alcohol portion having a higher alcohol concentration than that of the original azeotropic mixture; and an alcohol purification step of subjecting the separated alcohol portion to either a crystallization procedure or a distillation procedure to separate the alcohol portion into a low-alcohol portion having a lower alcohol concentration than that of the original alcohol portion and a high-alcohol portion having a higher alcohol concentration than that of the original alcohol portion, and thereby collecting alcohol as the high-alcohol portion.


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