The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 8044196 B1

PDF
Full Text
Expired
Date of Patent:
Oct. 25, 2011

Filed:

Jul. 14, 2004
Applicants:

Jwalant A. Shastri, Noida, IN;

Akshat Bhatnagar, Noida, IN;

Rajesh K. Thaper, Noida, IN;

Sushil K. Dubey, Noida, IN;

Inventors:

Jwalant A. Shastri, Noida, IN;

Akshat Bhatnagar, Noida, IN;

Rajesh K. Thaper, Noida, IN;

Sushil K. Dubey, Noida, IN;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 243/10 (2006.01);
U.S. Cl.
CPC ...
Abstract

Disclosed is a process for producing pure form of 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5] benzodiazepine. The process comprises of reacting 2-(2-aminoanilino)-5-methylthiophene-3-carbonitrile with N-methyl piperazine in conjunction with N-methylpiperazine acid salt, to produce 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5] benzodiazepine. Also disclosed is a process for obtaining the Polymorphic Form I of 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5] benzodiazepine by crystallizing the crude 2-methyl-4-(4-methyl-1-piperazinyl)-10H-thieno[2,3-b][1,5] benzodiazepine in a mixture of solvents.


Find Patent Forward Citations

Shastri, Jwalant. (2011). Process for producing pure form of 2-methyl-4-(4-methyl-1-piperazinyl)-10h-thieno[2,3-b][1,5]benzodiazepine (U.S. Patent No. 8044196). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/8044196

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