The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 7825259 B1

PDF
Full Text
Expired
Date of Patent:
Nov. 02, 2010

Filed:

Apr. 25, 2007
Applicants:

Cláudia Cristiana Cassol, Porto Alegre, BR;

Bauer Costa Ferrera, Porto Alegre, BR;

Gunter Ebeling, Porto Alegre, BR;

Jairton Dupont, Porto Alegre, BR;

Inventors:

Cláudia Cristiana Cassol, Porto Alegre, BR;

Bauer Costa Ferrera, Porto Alegre, BR;

Gunter Ebeling, Porto Alegre, BR;

Jairton Dupont, Porto Alegre, BR;

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D 233/54 (2006.01); C07F 1/00 (2006.01);
U.S. Cl.
CPC ...
Abstract

The reaction of N-alkylimidazol with alkyl sulfonates, at room temperature, favors the production of 1,3-dialkylimidazolium alkane-sulfonates as crystalline solids at high yields. The alkane-sulfonate anions may be easily substituted by a series of other anions [BF, PF, PF(CFCF), CFSOand (CFSO)N] through simple anion, salt, or acid reactions in water at room temperature. The extraction with dichloromethane, filtration, and evaporation of the solvent, allows the production of the desired ionic liquids at a yield of 80-95%. The purity of these ionic liquids (in some cases >99.4%) is performed using the intensity ofC satellite signals from the magnetic resonance spectrums of the N-methyl imidazolium group as an internal standard.


Find Patent Forward Citations

Cassol, Cláudia. (2010). Method of preparation of halogen-free ionic liquids and ionic liquids prepared in this manner (U.S. Patent No. 7825259). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/7825259

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