The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 12, 2010

Filed:

Nov. 10, 2005
Applicants:

Lee Rigby, Richmond, KY (US);

R. Merritt Sink, Lake Jackson, TX (US);

Inventors:

Lee Rigby, Richmond, KY (US);

R. Merritt Sink, Lake Jackson, TX (US);

Assignee:

BASF SF, Ludwigshafen, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 38/52 (2006.01);
U.S. Cl.
CPC ...
Abstract

Platinum is applied on a carrier such as graphite to form a platinum catalyst. The catalyst becomes poisoned with a metal as a result of use of the catalyst in preparation of hydroxylammonium salts. A method of regenerating the catalyst dissolves the platinum and the metal in an acid. The method also adds ammonium sulfate to the acid to precipitate the platinum. The ammonium sulfate is a by-product of a commercial process to synthesize a caprolactam. Also, the method precipitates the platinum onto the carrier for reuse in the preparation of the hydroxylammonium salts and in preparation of the caprolactam.


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