The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 03, 2010

Filed:

Jun. 05, 2006
Applicants:

LI Deng, Newton, MA (US);

Jianfeng Hang, Champaign, IL (US);

Liang Tang, Waltham, MA (US);

Inventors:

Li Deng, Newton, MA (US);

Jianfeng Hang, Champaign, IL (US);

Liang Tang, Waltham, MA (US);

Assignee:

Brandeis University, Waltham, MA (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07D 453/04 (2006.01); C07D 453/00 (2006.01); C07C 59/11 (2006.01); C07D 413/12 (2006.01); C07C 229/12 (2006.01);
U.S. Cl.
CPC ...
Abstract

One aspect of the present invention relates to a method for the kinetic resolution of racemic and diastereomeric mixtures of chiral compounds. The critical elements of the method are: a non-racemic chiral tertiary-amine-containing catalyst; a racemic or diastereomeric mixture of a chiral substrate, e.g., a cyclic carbonate or cyclic carbamate; and a nucleophile, e.g., an alcohol, amine or thiol. A preferred embodiment of the present invention relates to a method for achieving the kinetic resolution of racemic and diastereomeric mixtures of derivatives of α- and β-amino, hydroxy, and thio carboxylic acids. In certain embodiments, the methods of the present invention achieve dynamic kinetic resolution of a racemic or diastereomeric mixture of a substrate, i.e., a kinetic resolution wherein the yield of the resolved enantiomer or diastereomer, respectively, exceeds the amount present in the original mixture due to the in situ equilibration of the enantiomers or diastereomers under the reaction conditions prior to the resolution step.


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