The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 10, 2009

Filed:

Jan. 26, 2006
Applicants:

Johnathan E. Holladay, Kennewick, WA (US);

Jianli HU, Kennewick, WA (US);

Yong Wang, Richland, WA (US);

Todd A. Werpy, West Richland, WA (US);

Inventors:

Johnathan E. Holladay, Kennewick, WA (US);

Jianli Hu, Kennewick, WA (US);

Yong Wang, Richland, WA (US);

Todd A. Werpy, West Richland, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/00 (2006.01); C07D 315/00 (2006.01); C07D 493/00 (2006.01); C07H 1/00 (2006.01); C07H 17/00 (2006.01); C07H 5/04 (2006.01); C07H 1/06 (2006.01); C13K 5/00 (2006.01);
U.S. Cl.
CPC ...
Abstract

The invention includes methods for producing dianhydrosugar alcohol by providing an acid catalyst within a reactor and passing a starting material through the reactor at a first temperature. At least a portion of the staring material is converted to a monoanhydrosugar isomer during the passing through the column. The monoanhydrosugar is subjected to a second temperature which is greater than the first to produce a dianhydrosugar. The invention includes a method of producing isosorbide. An initial feed stream containing sorbitol is fed into a continuous reactor containing an acid catalyst at a temperature of less than 120° C. The residence time for the reactor is less than or equal to about 30 minutes. Sorbitol converted to 1,4-sorbitan in the continuous reactor is subsequently provided to a second reactor and is dehydrated at a temperature of at least 120° C. to produce isosorbide.


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