The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 29, 2009

Filed:

Mar. 04, 2004
Applicants:

Renate Patrascu, Stade, DE;

Sabrina Astori, Venice, IT;

Meinolf M. Weidenbach, Drochtersen, DE;

Inventors:

Renate Patrascu, Stade, DE;

Sabrina Astori, Venice, IT;

Meinolf M. Weidenbach, Drochtersen, DE;

Assignee:

Dow Global Technologies, Inc., Midland, MI (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 3/38 (2006.01); B01D 3/42 (2006.01); C07D 301/32 (2006.01);
U.S. Cl.
CPC ...
Abstract

A process of separating a purified propylene oxide from a crude epoxidation product produced, preferably, in an epoxidation reaction of propylene with hydrogen peroxide. The process involves removing bulk water, bulk methanol, and unreacted propylene from the crude epoxidation product and thereafter subjecting the resulting propylene oxide product to extractive distillation with water as an extraction solvent. Under distillation conditions, including a bottoms temperature of greater than about 55° C. and less than about 75° C., an overhead or side-cut distillate stream containing a purified propylene oxide is obtained with low yield loss of propylene oxide to propylene glycols and other glycol heavies. The purified propylene oxide can be further purified in a finishing distillation to obtain propylene oxide meeting commercial grade purity requirements.


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