The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 7585978 B1

PDF
Full Text
Expired
Date of Patent:
Sep. 08, 2009

Filed:

Nov. 28, 2006
Applicants:

Christopher N. Jobdevairakkam, Plainsboro, NJ (US);

Jayaraman Kannappan, Piscataway, NJ (US);

Inventors:

Christopher N. Jobdevairakkam, Plainsboro, NJ (US);

Jayaraman Kannappan, Piscataway, NJ (US);

Assignee:

Navinta LLC, Ewing, NJ (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D 213/803 (2006.01); C07D 401/00 (2006.01); C07D 211/68 (2006.01);
U.S. Cl.
CPC ...
Abstract

A process of preparing a stable parenteral solution of a 1,4-dihydropyridine salt, such as nicardipine hydrochloride, in an acidic aqueous medium. The presence of L-arginine in the solution enhances the solubility of the salt, which is poorly soluble in water. An aqueous, injectable isotonic solution at pH about 3.5-3.6 consists essentially of nicardipine hydrochloride, L-arginine, and a sugar alcohol. An improved single pot manufacturing process for obtaining unsymmetrical 1,4-dihydropyridines by using more than one mole equivalent of aldehyde with respect to the other reactants (amino crotonate and acetoacetate ester). The reaction can be conducted in a solvent present at 20 times the amount of any one component. A process for changing one polymorph of nicardipine hydrochloride (Form A) into another (Form B), and a separate process for the reverse (Form B into Form A).


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