The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 7491834 B1

PDF
Full Text
Expired
Date of Patent:
Feb. 17, 2009

Filed:

Apr. 08, 2003
Applicants:

Raymond Vincent Heavon Jones, Grangemouth, GB;

Alan John Whitton, Grangemouth, GB;

Colin John Bennie, Grangemouth, GB;

David John Ritchie, Grangemouth, GB;

Pascal Bugnon, Monthey, CH;

Inventors:

Raymond Vincent Heavon Jones, Grangemouth, GB;

Alan John Whitton, Grangemouth, GB;

Colin John Bennie, Grangemouth, GB;

David John Ritchie, Grangemouth, GB;

Pascal Bugnon, Monthey, CH;

Assignees:

Syngenta Crop Protection, Inc., Greensboro, NC (US);

Syngenta Limited, , GB;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07D 311/00 (2006.01);
U.S. Cl.
CPC ...
Abstract

3-Isochromanone is prepared by partially chlorinating o-tolylacetic acid with sulphuryl chloride or chlorine gas in an inert organic solvent in the presence of a free radical initiator. The 2-chloromethylphenylacetic acid first obtained is converted to 3-isochromanone by treatment with a base and separated from unreacted o-tolylacetic acid, which is in the form of a salt, by a phase separation technique. The separated o-tolylacetic acid salt is converted to o-tolylacetic acid by controlled acidification and the o-tolylacetic acid is extracted for re-use. The invention reduces the formation of unwanted, over-chlorinated by-products and leads to a more efficient process.


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Jones, Raymond Vincent Heavon. (2009). Chemical process (U.S. Patent No. 7491834). U.S. Patent and Trademark Office. https://idiyas.com/patent/badge/7491834

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