The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 25, 2008

Filed:

Oct. 04, 2006
Applicants:

Masafumi Watanabe, Okayama, JP;

Junichi Amemiya, Okayama, JP;

Ikutaro Kuzuhara, Okayama, JP;

Inventors:

Masafumi Watanabe, Okayama, JP;

Junichi Amemiya, Okayama, JP;

Ikutaro Kuzuhara, Okayama, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 319/06 (2006.01);
U.S. Cl.
CPC ...
Abstract

A process of producing 2-(5-ethyl-5-hydroxymethyl-1,3-dioxane-2-yl)-2-methylpropane-1-ol (DOG) by the acetalization of hydroxypivalaldehyde with trimethylolpropane in water in the presence of an acid catalyst and optional seed crystals. DOG crystals having an increased particle size and containing the trans isomer in a high content are produced by the process in which the reaction temperature, pH of the reaction system and concentration of DOG to be produced in the reaction system are controlled.


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