The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 11, 2007

Filed:

Apr. 08, 2005
Applicants:

Randi Wright Wytcherley, Belgrade, MT (US);

Tai-li Chou, Bozeman, MT (US);

Inventors:

Randi Wright Wytcherley, Belgrade, MT (US);

Tai-Li Chou, Bozeman, MT (US);

Assignee:

GTC Technology, Inc., Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/42 (2006.01);
U.S. Cl.
CPC ...
Abstract

A method and apparatus for purifying carboxylic acids is disclosed. A mixture containing crude carboxylic acid is contacted with a selective crystallization solvent to form a slurry of a salt complex of the carboxylic acid and the selective crystallization solvent. The salt complex is recovered and optionally processed to recover the free carboxylic acid. The method and apparatus of the invention is particularly suitable for purifying aromatic dicarboxylic acids such as terephthalic acid. The present invention also reduces contamination by carboxybenaldehyde isomers in crude phthalic acids by oxidizing the carboxybenzaldehyde to the corresponding phthalic acid.


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